sample: 13C15N EfR36.003 conc: 0.87 mM buffer: 20 mM MES, 100 mM NaCl, 5 mM CaCl2 10 mM DTT, 5% D2O pH 6.5 prepared by: Rong experiment: 3D CCcoNH tocsy 28.5 h instrument: INOVA 600 probe 4477 acquired by: jma/AB 03-19-04 T=20C ncyc=3