# 1 "/opt/topspin/exp/stan/nmr/lists/pp/hmbcgplpndqf" ;hmbcgplpndqf ;avance-version (07/04/04) ;HMBC ;2D H-1/X correlation via heteronuclear zero and double quantum ; coherence ;optimized on long range couplings ;with low-pass J-filter to suppress one-bond correlations ;no decoupling during acquisition ;using gradient pulses for selection ; ;$CLASS=HighRes ;$DIM=2D ;$TYPE= ;$SUBTYPE= ;$COMMENT= # 1 "/opt/topspin/exp/stan/nmr/lists/pp/Avance.incl" 1 ;Avance3.incl ; for AV III ; ;avance-version (07/12/14) ; ;$CLASS=HighRes Incl ;$COMMENT= ;$Id: Avance3.incl,v 1.6.2.2 2007/12/14 16:06:46 ber Exp $ # 18 "/opt/topspin/exp/stan/nmr/lists/pp/hmbcgplpndqf" 2 # 1 "/opt/topspin/exp/stan/nmr/lists/pp/Grad.incl" 1 ;Grad2.incl - include file for Gradient Spectroscopy ; for 1 ; ;avance-version (07/01/17) ; ;$CLASS=HighRes Incl ;$COMMENT= define list EA= ;$Id: Grad2.incl,v 1.12 2007/01/22 14:22:35 ber Exp $ # 19 "/opt/topspin/exp/stan/nmr/lists/pp/hmbcgplpndqf" 2 "p2=p1*2" "d2=1s/(cnst2*2)" "d6=1s/(cnst13*2)" "d0=3u" "in0=inf1/2" # 1 "mc_line 32 file /opt/topspin/exp/stan/nmr/lists/pp/hmbcgplpndqf expanding definition part of mc command before ze" define delay MCWRK define delay MCREST "MCWRK = 0.500000*d1" "MCREST = d1 - d1" dccorr # 32 "/opt/topspin/exp/stan/nmr/lists/pp/hmbcgplpndqf" 1 ze # 1 "mc_line 32 file /opt/topspin/exp/stan/nmr/lists/pp/hmbcgplpndqf expanding definition of mc command after ze" # 33 "/opt/topspin/exp/stan/nmr/lists/pp/hmbcgplpndqf" # 1 "mc_line 33 file /opt/topspin/exp/stan/nmr/lists/pp/hmbcgplpndqf expanding start label for mc command" 2 MCWRK LBLF1, MCWRK MCREST # 34 "/opt/topspin/exp/stan/nmr/lists/pp/hmbcgplpndqf" 3 p1 ph1 d2 p3:f2 ph3 d6 p3:f2 ph4 d0 50u setnmr3|0 setnmr0|34|32|33 ctrlgrad 0 p16:gp1 d16 p2 ph2 50u p16:gp2 d16 d0 p3:f2 ph5 4u p16:gp3 d16 4u setnmr3^0 setnmr0^34^32^33 ctrlgrad 7 go=2 ph31 # 1 "mc_line 54 file /opt/topspin/exp/stan/nmr/lists/pp/hmbcgplpndqf expanding mc command in line" MCWRK wr #0 if #0 zd id0 lo to LBLF1 times td1 MCWRK # 55 "/opt/topspin/exp/stan/nmr/lists/pp/hmbcgplpndqf" exit ph1=0 ph2=0 0 0 0 2 2 2 2 ph3=0 0 2 2 ph4=0 2 ph5=0 0 0 0 0 0 0 0 2 2 2 2 2 2 2 2 ph31=0 2 0 2 0 2 0 2 2 0 2 0 2 0 2 0 ;pl1 : f1 channel - power level for pulse (default) ;pl2 : f2 channel - power level for pulse (default) ;p1 : f1 channel - 90 degree high power pulse ;p2 : f1 channel - 180 degree high power pulse ;p3 : f2 channel - 90 degree high power pulse ;p16: homospoil/gradient pulse ;d0 : incremented delay (2D) [3 usec] ;d1 : relaxation delay; 1-5 * T1 ;d2 : 1/(2J)XH ;d6 : delay for evolution of long range couplings ;d16: delay for homospoil/gradient recovery ;cnst2: = J(XH) ;cnst13: = J(XH) long range ;inf1: 1/SW(X) = 2 * DW(X) ;in0: 1/(2 * SW(X)) = DW(X) ;nd0: 2 ;NS: 2 * n ;DS: 16 ;td1: number of experiments ;FnMODE: QF ;use gradient ratio: gp 1 : gp 2 : gp 3 ; 50 : 30 : 40.1 for C-13 ; 70 : 30 : 50.1 for N-15 ;for z-only gradients: ;gpz1: 50% for C-13, 70% for N-15 ;gpz2: 30% ;gpz3: 40.1% for C-13, 50.1% for N-15 ;use gradient files: ;gpnam1: SINE.100 ;gpnam2: SINE.100 ;gpnam3: SINE.100 ;$Id: hmbcgplpndqf,v 1.4 2007/04/11 13:34:29 ber Exp $