sample: 13C15N ER111 conc: 1.3 mM buffer: 20 mM NH4OAc, 100 mM NaCl, 5mM CaCl2, 5 mM DTT, 5% D2O 0.02% NaN3 pH 5.5 prepared by: Rong experiment: 3D - H-HACANH - 16 hr instrument: INOVA 600 probe 4477 acquired by: pkr 08-27-02 pfg_H_hacanh_se2